Izvestiya of Saratov University.

Chemistry. Biology. Ecology

ISSN 1816-9775 (Print)
ISSN 2541-8971 (Online)


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Russian
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Article type: 
Article
UDC: 
636.085.3:577.18:543

Rapid Determination of Tetracyclines in Milk by the Method of Mass Spectrometry High Resolution

Autors: 
Amelin V. G., Vladimir State University
Amelin A. I., Vladimir State University
Abstract: 

The method of determination of tetracycline antibiotics (tetracycline, chlortetracycline, oxytetracycline, doxycycline) in the milk of methods HPLC-MS/MS/MS and HPLC-QTOF-MS, with a simple and rapid sample preparation. The ranges defined concentrations of tetracyclines in milk sample of 1 g was 1–200 ?g/kg. Relative standard deviation of the results of the analysis does not exceed 7%. The analysis duration 30–40 minutes.

Reference: 

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Received: 
23.01.2015
Accepted: 
02.04.2015
Published: 
05.06.2015